Chem. Commun., 2013, Accepted Manuscript
DOI: 10.1039/C3CC45175E, Communication
DOI: 10.1039/C3CC45175E, Communication
Ajai Kumar Singh, Kamal Nayan Sharma, Hemant Joshi, Alpesh Kumar Sharma, Om Prakash
The PdTe NPs(hexagonal) and nanorods(first example) have been synthesized for the first time from single source precursors(SSPs), [Pd(L1)Cl2](1) and [Pd(L2)Cl]BF4(2) [L1, 4-bromo-1-[2-(4-methoxyphenyltellanyl)ethyl]-1H-pyrazole; L2, bis-[2-(4-bromopyrazol-1-yl)ethyl]telluride] by their thermolysis in OA-ODE mixture(1:1) and TOP respectively. The composition of PdTe phase does not change with SSP/solvent. The complex 2 gives small size nanostructures.
The content of this RSS Feed (c) The Royal Society of Chemistry
The PdTe NPs(hexagonal) and nanorods(first example) have been synthesized for the first time from single source precursors(SSPs), [Pd(L1)Cl2](1) and [Pd(L2)Cl]BF4(2) [L1, 4-bromo-1-[2-(4-methoxyphenyltellanyl)ethyl]-1H-pyrazole; L2, bis-[2-(4-bromopyrazol-1-yl)ethyl]telluride] by their thermolysis in OA-ODE mixture(1:1) and TOP respectively. The composition of PdTe phase does not change with SSP/solvent. The complex 2 gives small size nanostructures.
The content of this RSS Feed (c) The Royal Society of Chemistry